2WAT
Structure of the fungal type I FAS PPT domain in complex with CoA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-08-20 |
Detector | ADSC CCD |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 145.587, 73.764, 105.689 |
Unit cell angles | 90.00, 130.80, 90.00 |
Refinement procedure
Resolution | 80.010 - 2.200 |
R-factor | 0.219 |
Rwork | 0.217 |
R-free | 0.25200 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.040 |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 80.000 | 2.320 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.100 | 0.400 |
Number of reflections | 43185 | |
<I/σ(I)> | 7.8 | 2.3 |
Completeness [%] | 97.9 | 89 |
Redundancy | 3.7 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4 | pH 4 |