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2W7F

Crystal structure of Y51FbsSHMT L-Ser external aldimine

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RU200
Temperature [K]100
Detector technologyIMAGE PLATE
DetectorMARRESEARCH
Spacegroup nameP 21 21 2
Unit cell lengths61.010, 106.510, 57.170
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution22.450 - 1.670
R-factor0.182
Rwork0.180
R-free0.21100
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1kl1
RMSD bond length0.012
RMSD bond angle1.331
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareREFMAC
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0001.720
High resolution limit [Å]1.6601.660
Rmerge0.0600.450
Number of reflections43037
<I/σ(I)>24.83.8
Completeness [%]96.583.7
Redundancy20.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
150% MPD, 0.1 M HEPES PH 7.5, 0.2 MM EDTA, 5 MM 2-MERCAPTOETHANOL, 10 MM L-SER

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PDB entries from 2024-05-15

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