2W66
BtGH84 in complex with HQ602
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-05-09 |
Detector | ADSC CCD |
Spacegroup name | P 1 |
Unit cell lengths | 51.199, 93.465, 99.010 |
Unit cell angles | 104.16, 94.01, 103.02 |
Refinement procedure
Resolution | 95.350 - 2.270 |
R-factor | 0.19 |
Rwork | 0.188 |
R-free | 0.23600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vvn |
RMSD bond length | 0.015 |
RMSD bond angle | 1.596 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.4.0077) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 95.350 | 2.390 |
High resolution limit [Å] | 2.270 | 2.270 |
Rmerge | 0.080 | 0.430 |
Number of reflections | 76272 | |
<I/σ(I)> | 9.7 | 2.6 |
Completeness [%] | 96.0 | 94.7 |
Redundancy | 2.2 | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.3M NH4AC 10% GLYCEROL 15% PEG3350 0.1M MES PH6 |