2W44
Structure DeltaA1-A4 insulin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I911-3 |
Synchrotron site | MAX II |
Beamline | I911-3 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-02-05 |
Detector | MARRESEARCH |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 41.050, 88.620, 73.760 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.340 - 2.000 |
R-factor | 0.208 |
Rwork | 0.205 |
R-free | 0.25800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7ins |
RMSD bond length | 0.016 |
RMSD bond angle | 1.571 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0053) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.000 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.040 | 0.200 |
Number of reflections | 8261 | |
<I/σ(I)> | 24.1 | 7 |
Completeness [%] | 87.6 | 53.5 |
Redundancy | 5.7 | 5.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 150 MM NA/K-PHOSPHATE PH 7.0 AND 7.5 % (V/V) ETHANOL |