2W2M
WT PCSK9-DELTAC BOUND TO WT EGF-A OF LDLR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-01-31 |
Detector | ADSC CCD |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 83.004, 83.004, 211.566 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.000 - 2.400 |
R-factor | 0.21719 |
Rwork | 0.215 |
R-free | 0.25421 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2qtw |
RMSD bond length | 0.007 |
RMSD bond angle | 1.228 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.000 | 2.530 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.130 | 0.680 |
Number of reflections | 29902 | |
<I/σ(I)> | 13.4 | 2.1 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 6.4 | 5.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 0.1M HEPES PH 7.5, 10% (V/V) 2-PROPANOL, 20% (W/V) PEG 4000 |