2VXW
Structural and Functional Studies of the Potent Anti-HIV Chemokine Variant P2-RANTES
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 HF |
| Temperature [K] | 287 |
| Detector | RIGAKU MICROMAX |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 116.678, 51.982, 61.692 |
| Unit cell angles | 90.00, 117.87, 90.00 |
Refinement procedure
| Resolution | 50.000 - 1.700 |
| R-factor | 0.2173 |
| Rwork | 0.217 |
| R-free | 0.24800 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.562 |
| Data reduction software | CNS |
| Data scaling software | HKL-2000 |
| Refinement software | CNS (1.0) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 1.700 |
| Rmerge | 0.050 |
| Number of reflections | 34463 |
| <I/σ(I)> | 12 |
| Completeness [%] | 97.4 |
| Redundancy | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5.5 | pH 5.5 |
