2VSZ
Crystal Structure of the ELMO1 PH domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-02-20 |
Detector | ADSC CCD |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 166.016, 166.016, 81.704 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 144.340 - 2.300 |
R-factor | 0.209 |
Rwork | 0.208 |
R-free | 0.23900 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.021 |
RMSD bond angle | 1.944 |
Data reduction software | MOSFLM |
Data scaling software | SCALEPACK |
Phasing software | SHELXCDE |
Refinement software | REFMAC (5.4.0066) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.420 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.060 | 0.230 |
Number of reflections | 29960 | |
<I/σ(I)> | 22.7 | 8.3 |
Completeness [%] | 99.9 | 100 |
Redundancy | 6.3 | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.75 | 2.1 M SODIUM MALONATE [PH 6.75] |