Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 1991-08-04 |
| Detector | RIGAKU IMAGE PLATE |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 113.950, 113.950, 138.050 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 15.660 - 2.710 |
| R-factor | 0.174 |
| Rwork | 0.171 |
| R-free | 0.23400 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2ace |
| RMSD bond length | 0.030 |
| RMSD bond angle | 2.651 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | PROTIN |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 15.660 | 2.780 |
| High resolution limit [Å] | 2.800 | 2.710 |
| Rmerge | 0.150 | |
| Number of reflections | 26435 | |
| Completeness [%] | 97.5 | |
| Redundancy | 4.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
