2VOJ
Ternary complex of M. tuberculosis Rv2780 with NAD and pyruvate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Detector | MARRESEARCH |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 88.993, 88.993, 373.855 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 377.960 - 2.600 |
R-factor | 0.18886 |
Rwork | 0.187 |
R-free | 0.22998 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.015 |
RMSD bond angle | 1.835 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.920 | 2.690 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.070 | 0.240 |
Number of reflections | 46674 | |
<I/σ(I)> | 30.3 | 7.9 |
Completeness [%] | 98.0 | 99.2 |
Redundancy | 7 | 5.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |