2VL8
CRYSTAL STRUCTURE OF THE CATALYTIC DOMAIN OF LETHAL TOXIN FROM CLOSTRIDIUM SORDELLII IN COMPLEX WITH UDP, CASTANOSPERMINE AND CALCIUM ION
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 57.689, 191.332, 205.384 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 95.780 - 2.310 |
R-factor | 0.218 |
Rwork | 0.217 |
R-free | 0.25500 |
Structure solution method | OTHER |
RMSD bond length | 0.014 |
RMSD bond angle | 1.372 |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 95.780 | |
High resolution limit [Å] | 2.310 | 2.310 |
Rmerge | 0.160 | 0.440 |
Number of reflections | 100405 | |
<I/σ(I)> | 11 | 5.2 |
Completeness [%] | 99.6 | 98.9 |
Redundancy | 8 | 8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |