2VG3
Rv2361 with citronellyl pyrophosphate
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Spacegroup name | P 32 |
| Unit cell lengths | 86.870, 86.870, 184.070 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 75.160 - 1.800 |
| R-factor | 0.204 |
| Rwork | 0.203 |
| R-free | 0.23100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.264 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 5.000 | 1.800 |
| High resolution limit [Å] | 1.800 | 1.700 |
| Rmerge | 0.070 | 0.420 |
| Number of reflections | 134070 | |
| <I/σ(I)> | 12 | 2 |
| Completeness [%] | 93.0 | 92 |
| Redundancy | 2.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
