2V92

Crystal structure of the regulatory fragment of mammalian AMPK in complexes with ATP-AMP

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	100
Detector technology	IMAGE PLATE
Spacegroup name	P 21 21 21
Unit cell lengths	48.961, 121.032, 127.247
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 - 2.400
Rwork	0.217
R-free	0.25900
Structure solution method	MOLECULAR REPLACEMENT
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	2.400
Rmerge	0.100
Number of reflections	30415
<I/σ(I)>	14.8
Completeness [%]	99.7
Redundancy	9.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1