2V8I

Structure of a Family 2 Pectate Lyase in a Native Form

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	113
Spacegroup name	P 21 21 21
Unit cell lengths	58.486, 95.642, 126.608
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.590 - 1.500
R-factor	0.223
Rwork	0.222
R-free	0.24300
Structure solution method	SIRAS
Starting model (for MR)	NONE
RMSD bond length	0.009
RMSD bond angle	1.144
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	19.590
High resolution limit [Å]	1.500
Rmerge	0.050
Number of reflections	105592
Completeness [%]	97.4
Redundancy	3.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1