2V79
Crystal Structure of the N-terminal domain of DnaD from Bacillus Subtilis
Experimental procedure
Experimental method | MAD |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 93 |
Detector technology | IMAGE PLATE |
Collection date | 2006-05-27 |
Detector | RIGAKU IMAGE-PLATE |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 78.666, 78.666, 124.558 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.000 - 2.000 |
R-factor | 0.182 |
Rwork | 0.181 |
R-free | 0.21000 |
Structure solution method | MAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.012 |
RMSD bond angle | 1.126 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHARP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.000 | 2.100 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.050 | 0.380 |
Number of reflections | 30662 | |
<I/σ(I)> | 24.4 | 4 |
Completeness [%] | 99.8 | 100 |
Redundancy | 5.8 | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.1M SODIUMACETATE, 3.2M SODIUMCHLORIDE |