2V2V
IspE in complex with ligand
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2006-10-24 |
Detector | RIGAKU IMAGE PLATE |
Spacegroup name | P 21 3 |
Unit cell lengths | 137.256, 137.256, 137.256 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 90.000 - 2.400 |
R-factor | 0.22 |
Rwork | 0.217 |
R-free | 0.27200 |
Structure solution method | OTHER |
RMSD bond length | 0.009 |
RMSD bond angle | 1.191 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | REFMAC |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 90.000 | 2.530 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.080 | 0.580 |
Number of reflections | 33908 | |
<I/σ(I)> | 15.8 | 2.5 |
Completeness [%] | 100.0 | 100 |
Redundancy | 5.5 | 5.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8 | 1.6 M (NH4)2SO4, 0.1 M NA CACODYLATE, PH 6.5, 0.1 M NABR |