2V11
Crystal Structure of Renin with Inhibitor 6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ENRAF-NONIUS FR571 |
Temperature [K] | 100 |
Detector technology | AREA DETECTOR |
Collection date | 1993-01-01 |
Detector | DELFT INSTRUMENTS |
Spacegroup name | P 21 3 |
Unit cell lengths | 142.900, 142.900, 142.900 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 3.100 |
R-factor | 0.217 |
Rwork | 0.217 |
Structure solution method | OTHER |
RMSD bond length | 0.019 |
RMSD bond angle | 3.673 |
Data reduction software | MADNESS |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 10.000 |
High resolution limit [Å] | 3.100 |
Rmerge | 0.220 |
Number of reflections | 17263 |
Completeness [%] | 96.0 |
Redundancy | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 3 | pH 3.00 |