2V01
Recombinant vertebrate calmodulin complexed with Pb
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I911-2 |
Synchrotron site | MAX II |
Beamline | I911-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | P 1 |
Unit cell lengths | 24.580, 29.950, 53.610 |
Unit cell angles | 88.57, 87.03, 82.95 |
Refinement procedure
Resolution | 20.000 - 2.150 |
R-factor | 0.191 |
Rwork | 0.188 |
R-free | 0.25300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1up5 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.298 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.250 |
High resolution limit [Å] | 2.150 | 2.150 |
Rmerge | 0.080 | 0.250 |
Number of reflections | 7838 | |
<I/σ(I)> | 8.2 | 4.3 |
Completeness [%] | 95.2 | 90.2 |
Redundancy | 2.2 | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4 | 40-50%MPD, PH4 |