Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-1 |
| Synchrotron site | ESRF |
| Beamline | ID14-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-07-05 |
| Detector | ADSC CCD |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 63.789, 110.753, 73.034 |
| Unit cell angles | 90.00, 109.86, 90.00 |
Refinement procedure
| Resolution | 69.010 - 2.500 |
| R-factor | 0.223 |
| Rwork | 0.220 |
| R-free | 0.27500 |
| Structure solution method | SAD |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.341 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SHELX |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 60.000 | 2.540 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Rmerge | 0.140 | 0.270 |
| Number of reflections | 33042 | |
| <I/σ(I)> | 0.14 | 2.8 |
| Completeness [%] | 99.0 | 99.3 |
| Redundancy | 4.4 | 4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6 | 287 | PEG 2000, LITHIUM CHLORIDE, DTT, REMARK 280 MES, PH 6.0, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 287.0 K |
