2UYZ
Non-covalent complex between Ubc9 and SUMO1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-06-18 |
Detector | ADSC CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 49.481, 35.030, 72.915 |
Unit cell angles | 90.00, 93.41, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.480 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.060 | 0.230 |
Number of reflections | 49557 | |
<I/σ(I)> | 6.3 | 1.6 |
Completeness [%] | 99.2 | 99.3 |
Redundancy | 3.5 | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | 16.5 % (W/V) PEG3350 100 MM BISTRIS PH 5.5 15 % (W/V) GLYCEROL |