2UYP
Crystal structure of E. coli TdcF with bound propionate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2002-07-11 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 72.435, 85.744, 62.512 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.580 - 2.440 |
R-factor | 0.171 |
Rwork | 0.166 |
R-free | 0.25300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1qu9 |
RMSD bond length | 0.021 |
RMSD bond angle | 1.843 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.250 | 2.540 |
High resolution limit [Å] | 2.450 | 2.450 |
Rmerge | 0.080 | 0.300 |
Number of reflections | 14818 | |
<I/σ(I)> | 12.49 | 2.58 |
Completeness [%] | 98.9 | 94 |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 10% PEG 1000, 8% PEG 8000, NO BUFFER, pH 7.00 |