2TCI
X-RAY CRYSTALLOGRAPHIC STUDIES ON HEXAMERIC INSULINS IN THE PRESENCE OF HELIX-STABILIZING AGENTS, THIOCYANATE, METHYLPARABEN AND PHENOL
Replaces: 1TCIExperimental procedure
| Spacegroup name | H 3 |
| Unit cell lengths | 80.640, 80.640, 37.520 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 10.000 - 1.800 |
| R-factor | 0.1975 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 0.033 |
| Refinement software | PROLSQ |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 5.640 * | |
| High resolution limit [Å] | 1.800 * | 1.800 * |
| Rmerge | 0.040 * | |
| Total number of observations | 11175 * | |
| Number of reflections | 7807 * | |
| Completeness [%] | 92.4 * | 51.2 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | hydrochrolic acid | 0.02 (M) |
