2RKU
Structure of PLK1 in complex with BI2536
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Detector technology | CCD |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.0 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 66.593, 66.593, 154.110 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 33.410 - 1.950 |
R-factor | 0.192 |
Rwork | 0.190 |
R-free | 0.24100 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.438 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.020 |
High resolution limit [Å] | 1.950 | 4.200 | 1.950 |
Rmerge | 0.069 | 0.044 | 0.505 |
Number of reflections | 29527 | ||
<I/σ(I)> | 12.7 | ||
Completeness [%] | 99.9 | 99.1 | 99.9 |
Redundancy | 6.6 | 6.8 | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |