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2RKU

Structure of PLK1 in complex with BI2536

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 17-ID
Synchrotron siteAPS
Beamline17-ID
Detector technologyCCD
DetectorADSC QUANTUM 210
Wavelength(s)1.0
Spacegroup nameP 32 2 1
Unit cell lengths66.593, 66.593, 154.110
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution33.410 - 1.950
R-factor0.192
Rwork0.190
R-free0.24100
RMSD bond length0.014
RMSD bond angle1.438
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]50.00050.0002.020
High resolution limit [Å]1.9504.2001.950
Rmerge0.0690.0440.505
Number of reflections29527
<I/σ(I)>12.7
Completeness [%]99.999.199.9
Redundancy6.66.86
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1

226707

PDB entries from 2024-10-30

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