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2R4V

Structure of human CLIC2, crystal form A

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 14-ID-B
Synchrotron siteAPS
Beamline14-ID-B
Temperature [K]100
Detector technologyCCD
DetectorADSC QUANTUM 315
Wavelength(s)0.9
Spacegroup nameP 21 21 21
Unit cell lengths44.015, 74.722, 79.827
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution54.550 - 1.850
R-factor0.21665
Rwork0.215
R-free0.25038
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1k0m
RMSD bond length0.016
RMSD bond angle1.538
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Phasing softwareAMoRE
Refinement softwareREFMAC (5.2.0005)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]54.5501.920
High resolution limit [Å]1.8501.850
Rmerge0.0600.300
Number of reflections23144
<I/σ(I)>31.32.8
Completeness [%]93.962
Redundancy10.54.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION829335%-50% PEG 400, 100mM Tris-HCl, pH8.0, 5mM GSH, VAPOR DIFFUSION, temperature 293K

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