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2R35

Crystal structure of RB human arg-insulin

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RU300
Temperature [K]298
Detector technologyIMAGE PLATE
Collection date2007-03-30
DetectorMAR scanner 345 mm plate
Wavelength(s)1.5418
Spacegroup nameH 3
Unit cell lengths80.522, 80.522, 38.329
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution25.790 - 2.080
R-factor0.2431
Rwork0.237
R-free0.29842
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1trz
RMSD bond length0.108
RMSD bond angle7.670
Data reduction softwareAUTOMAR
Phasing softwareAMoRE
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.110
High resolution limit [Å]2.0402.040
Rmerge0.2400.650
Number of reflections4169
<I/σ(I)>2.20.8
Completeness [%]70.352
Redundancy1.31.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.7293Sodium Citrate, Acetone, Rubidium Chloride, pH 6.7, VAPOR DIFFUSION, HANGING DROP, temperature 293K

217705

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