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2R34

Crystal structure of MN human arg-insulin

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RU300
Temperature [K]298
Detector technologyIMAGE PLATE
Collection date2007-03-25
DetectorMAR scanner 345 mm plate
Wavelength(s)1.5418
Spacegroup nameH 3
Unit cell lengths80.687, 80.687, 37.517
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution40.360 - 2.250
R-factor0.193
Rwork0.186
R-free0.26400
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1trz
RMSD bond length0.037
RMSD bond angle2.611
Data reduction softwareAUTOMAR
Phasing softwareAMoRE
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.290
High resolution limit [Å]2.2502.250
Rmerge0.1500.590
Number of reflections4331
<I/σ(I)>3.31
Completeness [%]96.395.3
Redundancy4.94.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.7293Sodium Citrate, Ammonium Sulphate, Magnesium Chloride, pH 6.7, VAPOR DIFFUSION, HANGING DROP, temperature 293K

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