2QYI
Crystal structure of a binary complex between an engineered trypsin inhibitor and Bovine trypsin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2006-08-16 |
Detector | MAR scanner 345 mm plate |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 143.694, 77.437, 72.907 |
Unit cell angles | 90.00, 103.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.600 |
Rwork | 0.208 |
R-free | 0.26800 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.544 |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.600 |
Rmerge | 0.088 |
Number of reflections | 23234 |
<I/σ(I)> | 4 |
Redundancy | 2.91 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 30% Jefamine, VAPOR DIFFUSION, temperature 293K |