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2QUF

Crystal Structure of Transcription Factor AXXA-PF0095 from Pyrococcus furiosus

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 22-BM
Synchrotron siteAPS
Beamline22-BM
Temperature [K]100
Detector technologyCCD
Collection date2007-06-14
DetectorMARMOSAIC 225 mm CCD
Wavelength(s)1.0
Spacegroup nameP 1 21 1
Unit cell lengths39.747, 93.484, 71.062
Unit cell angles90.00, 102.44, 90.00
Refinement procedure
Resolution32.530 - 2.800
R-factor0.246
Rwork0.244
R-free0.28100
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2plz
RMSD bond length0.007
RMSD bond angle1.058
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]32.5302.880
High resolution limit [Å]2.8002.800
Number of reflections11712
Completeness [%]98.085
Redundancy6.65.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
14.829170mM Sodium Acetate, 30% Glycerol, pH 4.8, modified microbatch, temperature 291K

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