2QIU
Structure of Human Arg-Insulin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 2006-08-31 |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | H 3 |
Unit cell lengths | 80.491, 80.491, 37.640 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.260 - 2.000 |
R-factor | 0.2026 |
Rwork | 0.197 |
R-free | 0.24931 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1zni |
RMSD bond length | 0.087 |
RMSD bond angle | 2.101 |
Data reduction software | AUTOMAR |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.260 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.120 | 0.440 |
Number of reflections | 6141 | |
<I/σ(I)> | 3.4 | 1.2 |
Completeness [%] | 100.0 | 100 |
Redundancy | 5 | 4.86 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.7 | 293 | Sodium Citrate, Acetone, Zinc Sulphate, pH 6.7, VAPOR DIFFUSION, HANGING DROP, temperature 293K |