2QCJ
Native Structure of Lyp
Experimental procedure
Experimental method | LAUE |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 200 |
Detector technology | IMAGE PLATE |
Collection date | 2005-09-20 |
Detector | RIGAKU RAXIS |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.309, 93.953, 148.173 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 3.000 |
R-factor | 0.287 |
Rwork | 0.284 |
R-free | 0.30700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1pxh |
RMSD bond length | 0.009 |
RMSD bond angle | 1.620 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.110 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.093 | 0.425 |
Number of reflections | 12511 | |
<I/σ(I)> | 15.9 | 3.5 |
Completeness [%] | 92.2 | 86.67 |
Redundancy | 5.5 | 5.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 5.6 | 293 | 20% PEG 3350, pH 5.6, EVAPORATION, temperature 293K |