Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-08-05 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1.008 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 141.248, 141.248, 211.705 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.080 - 2.700 |
R-factor | 0.20434 |
Rwork | 0.202 |
R-free | 0.25329 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | GGPS1 MONOMER BUILT INTO SAD-PHASED MAP (UNPUBLISHED) |
RMSD bond length | 0.014 |
RMSD bond angle | 1.389 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.080 | 2.720 |
High resolution limit [Å] | 2.700 | 2.700 |
Number of reflections | 59513 | |
<I/σ(I)> | 12 | 2.83 |
Completeness [%] | 99.9 | 100 |
Redundancy | 7.7 | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 293 | 25% PEG 3350, 0.2M MG FORMATE, pH 5.50, VAPOR DIFFUSION, SITTING DROP, temperature 293K |