2PZ1
Crystal Structure of Auto-inhibited Asef
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-02-12 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | .97925, .97936, .97164 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 100.418, 79.883, 67.407 |
Unit cell angles | 90.00, 122.99, 90.00 |
Refinement procedure
Resolution | 15.000 - 2.250 |
R-factor | 0.22063 |
Rwork | 0.217 |
R-free | 0.27925 |
Structure solution method | MAD, MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.063 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SHELXD |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.340 |
High resolution limit [Å] | 2.250 | 2.250 |
Number of reflections | 20993 | |
<I/σ(I)> | 30.2 | 3.23 |
Completeness [%] | 99.1 | 97.9 |
Redundancy | 2.8 | 2.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 291 | 100 mM HEPES pH 7, 20 % PEG 3350, 200 mM magnesium acetate, 10% glycerol, VAPOR DIFFUSION, SITTING DROP, temperature 291K |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 291 | 100 mM HEPES pH 7, 20 % PEG 3350, 200 mM magnesium acetate, 10% glycerol, VAPOR DIFFUSION, SITTING DROP, temperature 291K |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 291 | 100 mM HEPES pH 7, 20 % PEG 3350, 200 mM magnesium acetate, 10% glycerol, VAPOR DIFFUSION, SITTING DROP, temperature 291K |