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2PNC

Crystal Structure of Bovine Plasma Copper-Containing Amine Oxidase in Complex with Clonidine

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE BM16
Synchrotron siteESRF
BeamlineBM16
Temperature [K]100
Detector technologyCCD
Collection date2006-03-10
DetectorADSC QUANTUM 210
Wavelength(s)0.97984
Spacegroup nameP 21 21 21
Unit cell lengths78.360, 131.956, 134.159
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution29.110 - 2.400
R-factor0.23774
Rwork0.237
R-free0.25227
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1tu5
RMSD bond length0.004
RMSD bond angle0.877
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwareCNS
Refinement softwareREFMAC (5.2.0005)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]34.0002.530
High resolution limit [Å]2.4002.400
Rmerge0.1290.407
Number of reflections47787
<I/σ(I)>3.71.5
Completeness [%]86.882.1
Redundancy33.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION7.4293KH2PO4 (0.2 M, pH 7.4) and PEG 3350 (20%, w/v), VAPOR DIFFUSION, temperature 293K

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