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2PK8

Crystal structure of an uncharacterized protein PF0899 from Pyrococcus furiosus

Replaces:  1SHE
Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 22-ID
Synchrotron siteAPS
Beamline22-ID
Temperature [K]100
Detector technologyCCD
Collection date2003-11-16
DetectorMARMOSAIC 225 mm CCD
Wavelength(s)1.00000
Spacegroup nameP 32 2 1
Unit cell lengths47.080, 47.080, 83.950
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution19.810 - 1.850
R-factor0.2083
Rwork0.207
R-free0.24249
Structure solution methodMIRAS
RMSD bond length0.019
RMSD bond angle1.723
Data scaling softwareSCALEPACK
Phasing softwareSOLVE
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0001.920
High resolution limit [Å]1.8501.850
Number of reflections9476
Completeness [%]98.592.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP3.9291MODIFIED MICROBATCH USING 1 MICROLITER DROPS CONTAINING EQUAL VOLUMES OF PROTEIN CONCENTRATE (10 mg/mL) AND A PRECIPITANT SOLUTION CONTAINING 8% PEG 4000 IN 100mM SODIUM ACETATE, pH 3.9, TEMPERATURE 291K, VAPOR DIFFUSION, SITTING DROP

217705

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