2PAV
Ternary complex of Profilin-Actin with the Last Poly-Pro of Human VASP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 14-BM-C |
Synchrotron site | APS |
Beamline | 14-BM-C |
Temperature [K] | 200 |
Detector technology | CCD |
Collection date | 2005-12-19 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.90020 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 37.467, 75.460, 180.741 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.090 - 1.800 |
R-factor | 0.16 |
Rwork | 0.158 |
R-free | 0.20800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2btf |
RMSD bond length | 0.019 |
RMSD bond angle | 1.663 |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.076 | 0.345 |
Number of reflections | 47947 | |
<I/σ(I)> | 28.1 | 5.7 |
Completeness [%] | 98.1 | 97.7 |
Redundancy | 7 | 5.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 277.15 | 200 mM sodium formate, 20% PEG 3350, pH 7.4, VAPOR DIFFUSION, SITTING DROP, temperature 277.15K |