2P5B

The complex structure of JMJD2A and trimethylated H3K36 peptide

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 8.2.2
Synchrotron site	ALS
Beamline	8.2.2
Detector technology	CCD
Collection date	2006-08-08
Detector	ADSC QUANTUM 315
Spacegroup name	P 21 21 2
Unit cell lengths	100.915, 150.844, 57.346
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	47.340 - 1.990
Rwork	0.238
R-free	0.26300
Structure solution method	FOURIER SYNTHESIS
RMSD bond length	0.006
RMSD bond angle	1.200
Refinement software	CNS (1.1)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.000
Number of reflections	52214

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	EVAPORATION			EVAPORATION