2P24
I-Au/MBP125-135
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.1 |
Synchrotron site | ALS |
Beamline | 5.0.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-08-28 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.0 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 103.656, 103.656, 97.246 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.370 - 2.150 |
R-factor | 0.21138 |
Rwork | 0.209 |
R-free | 0.25996 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1k2d |
RMSD bond length | 0.022 |
RMSD bond angle | 1.734 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.400 | 2.230 |
High resolution limit [Å] | 2.150 | 2.150 |
Rmerge | 0.089 | 0.289 |
Number of reflections | 29462 | |
<I/σ(I)> | 18.7 | 5.99 |
Completeness [%] | 99.9 | |
Redundancy | 13.8 | 13.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 291.15 | 0.1 M NaOAc, 25% (w/v) PEG 1000, pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 291.15K |