2OXQ
Structure of the UbcH5 :CHIP U-box complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-08-07 |
Detector | NOIR-1 |
Wavelength(s) | 1.24 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 79.042, 93.399, 144.009 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.000 | 3.000 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.080 | 0.466 |
Number of reflections | 24283 | |
<I/σ(I)> | 8.5 | 1.6 |
Completeness [%] | 99.9 | 100 |
Redundancy | 3.4 | 3.42 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.7 | 293 | 1.65M Ammonium Sulfate, 0.09M Bistris, pH 6.7, VAPOR DIFFUSION, HANGING DROP, temperature 293K |