2OW1
MMP-9 active site mutant with trifluoromethyl hydroxamate inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MPG/DESY, HAMBURG BEAMLINE BW6 |
Synchrotron site | MPG/DESY, HAMBURG |
Beamline | BW6 |
Detector technology | CCD |
Collection date | 2005-03-11 |
Detector | MAR CCD 165 mm |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 55.720, 55.720, 260.450 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.790 - 2.200 |
R-factor | 0.217 |
Rwork | 0.217 |
R-free | 0.26700 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.100 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 99.000 | 2.180 |
High resolution limit [Å] | 2.150 | 2.150 |
Rmerge | 0.043 | 0.163 |
Number of reflections | 19793 | |
<I/σ(I)> | 16.3 | 3.5 |
Completeness [%] | 77.0 | 64.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |