2ON5
Structure of NaGST-2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2005-10-01 |
| Detector | RIGAKU RAXIS IV |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 57.916, 107.921, 166.990 |
| Unit cell angles | 90.00, 90.02, 90.00 |
Refinement procedure
| Resolution | 25.000 - 1.900 |
| R-factor | 0.1804 |
| Rwork | 0.178 |
| R-free | 0.22702 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1tw9 |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.408 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASES |
| Refinement software | REFMAC (5.2) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 33.000 | 1.890 |
| High resolution limit [Å] | 1.820 | 1.820 |
| Rmerge | 0.073 | 0.489 |
| Number of reflections | 142281 | |
| <I/σ(I)> | 13.1 | 1.39 |
| Completeness [%] | 88.1 | 50.7 |
| Redundancy | 2.9 | 1.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | PEG 4000, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
