2OKO
Z. mobilis tRNA guanine transglycosylase E235Q mutant apo-structure at pH 5.5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Detector technology | IMAGE PLATE |
Collection date | 2006-12-13 |
Detector | RIGAKU RAXIS IV |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 90.407, 65.194, 70.514 |
Unit cell angles | 90.00, 96.36, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.500 |
R-factor | 0.1256 |
Rwork | 0.125 |
R-free | 0.17390 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1y5x |
RMSD bond length | 0.011 |
RMSD bond angle | 0.030 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CNS |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.500 |
Rmerge | 0.122 |
Number of reflections | 210241 |
<I/σ(I)> | 33 |
Completeness [%] | 91.5 |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | pH 5.5 |