2OJ9
Structure of IGF-1R kinase domain complexed with a benzimidazole inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1999-06-19 |
Detector | RIGAKU |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 57.271, 44.289, 65.744 |
Unit cell angles | 90.00, 99.05, 90.00 |
Refinement procedure
Resolution | 13.210 - 2.000 |
R-factor | 0.217 |
Rwork | 0.214 |
R-free | 0.27600 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.017 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | BUSTER-TNT (1.9.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.091 | 0.240 |
Number of reflections | 21556 | |
<I/σ(I)> | 20.9 | 2.6 |
Completeness [%] | 96.5 | 78.2 |
Redundancy | 5.2 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 277 | VAPOR DIFFUSION, HANGING DROP, temperature 277K |