2NWS
Structural and mechanistic changes along an engineered path from metallo to non-metallo KDO8P synthase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Wavelength(s) | 1.54180 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 84.466, 84.466, 159.907 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.160 - 1.800 |
R-factor | 0.234 |
Rwork | 0.234 |
R-free | 0.26800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1fwn |
RMSD bond length | 0.007 |
RMSD bond angle | 1.600 |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 33.000 |
High resolution limit [Å] | 1.800 |
Rmerge | 0.128 |
Number of reflections | 61836 |
<I/σ(I)> | 3.4 |
Completeness [%] | 99.7 |
Redundancy | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |