Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE BW7B |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | BW7B |
| Wavelength(s) | 0.843 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 118.784, 63.021, 35.527 |
| Unit cell angles | 90.00, 92.24, 90.00 |
Refinement procedure
| Resolution | 7.990 - 1.643 |
| R-factor | 0.149 |
| Rwork | 0.148 |
| R-free | 0.16543 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1nvt |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.135 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | CNS |
| Refinement software | REFMAC (5.2) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 7.990 |
| High resolution limit [Å] | 1.600 |
| Number of reflections | 29404 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 298 | VAPOR DIFFUSION, SITTING DROP, temperature 298.0K |
