2NCK

CRYSTAL STRUCTURE OF MYXOCOCCUS XANTHUS NUCLEOSIDE DIPHOSPHATE KINASE AND ITS INTERACTION WITH A NUCLEOTIDE SUBSTRATE AT 2.0 ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	P 43 21 2
Unit cell lengths	63.500, 63.500, 158.000
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 * - 2.000
R-factor	0.17
Rwork	0.170
RMSD bond length	0.007
RMSD bond angle	1.418
Phasing software	X-PLOR
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	2.000 *
Rmerge	0.097 *
Number of reflections	21862 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	sodium acetate	0.3 (M)
2	1	drop	acetic acid	0.1 (M)
3	1	drop	EDTA	0.01 (M)
4	1	drop	PEG3350	13 (%)
5	1	reservoir	sodium acetate	0.3 (M)
6	1	reservoir	acetic acid	0.1 (M)
7	1	reservoir	PEG3350	16 (%)
8	1	reservoir	EDTA	0.01 (M)