2MHQ
Solution structure of the major factor VIII binding region on von Willebrand factor
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Varian | INOVA | Varian INOVA | 600 |
| 2 | Bruker | AVANCE III | Bruker Avance III | 500 |
| 3 | Bruker | AVANCE III | Bruker Avance III | 700 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 3D HNCO |
| 10 | 1 | 2 | 2D constant-time 1H-13C HSQC |
| 11 | 1 | 1 | 3D 1H-15N NOESY |
| 12 | 1 | 4 | 3D 1H-13C NOESY |
| 13 | 1 | 3 | {1H}15N steady-state NOE |
| 14 | 1 | 3 | 15N R1rho relaxation |
| 15 | 1 | 3 | 15N R1 relaxation |
| 16 | 1 | 5 | 15N R2-CPMG relaxation dispersion |
| 17 | 1 | 5 | 15N R2-CPMG relaxation dispersion |
| 18 | 1 | 6 | 2D IPAP-15N HSQC |
| 19 | 1 | 7 | 2D IPAP-15N HSQC |
| 2 | 1 | 1 | 3D HNCA |
| 20 | 1 | 8 | 2D IPAP-15N HSQC |
| 21 | 1 | 6 | 2D IPAP-E.COSY-15N HSQC |
| 22 | 1 | 8 | 2D IPAP-E.COSY-15N HSQC |
| 23 | 1 | 6 | 3D IPAP-HNCO(J-CA) |
| 24 | 1 | 8 | 3D IPAP-HNCO(J-CA) |
| 25 | 1 | 6 | 3D HN(CO)CA(J-CB) |
| 26 | 1 | 8 | 3D HN(CO)CA(J-CB) |
| 27 | 1 | 6 | 3D IPAP-(HA)CA(CO)NH |
| 28 | 1 | 8 | 3D IPAP-(HA)CA(CO)NH |
| 29 | 1 | 1 | 2D 1H-15N HSQC |
| 3 | 1 | 1 | 3D HN(CO)CA |
| 30 | 1 | 1 | 2D 1H-13C HSQC |
| 31 | 1 | 1 | 2D constant-time 1H-13C HSQC |
| 32 | 1 | 4 | 2D 1H-13C HSQC |
| 33 | 1 | 4 | 2D constant-time 1H-13C HSQC |
| 4 | 1 | 1 | 3D HNCACB |
| 5 | 1 | 1 | 3D 15N HSQC-NOESY-15N HSQC |
| 6 | 1 | 1 | 3D HN(CACO)NH |
| 7 | 1 | 1 | 3D (H)CC(CO)NH |
| 8 | 1 | 1 | 3D H(CCCO)NH |
| 9 | 1 | 1 | 3D HCCH-TOCSY |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 7.4 | ambient | 298 |
Conformers
| Conformers Calculated Total Number | 10 |
| Conformers Submitted Total Number | 10 |
