2LK3

U2/U6 Helix I

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	DMX	Bruker DMX	750
2	Varian	INOVA	Varian INOVA	600

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-1H NOESY
10	2	6	2D 1H-13C HSQC aromatic
11	2	6	2D 1H-13C HSQC aliphatic
12	1	3	2D HNN-COSY
13	2	4	3D HCCH-TOCSY
14	2	4	3D HCCH-COSY
2	2	2	2D 1H-1H NOESY
3	2	2	2D 1H-1H TOCSY
4	2	2	2D 1H-13C HSQC aromatic
5	2	2	2D 1H-13C HSQC aliphatic
6	1	3	2D 1H-15N HMQC
7	2	4	2D 1H-13C HSQC aromatic
8	2	4	2D 1H-13C HSQC aliphatic
9	1	5	2D 1H-15N HMQC

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	7	ambient	283
2	7	ambient	298

Conformers

Conformers Calculated Total Number	50
Conformers Submitted Total Number	10