2L4K
Water refined solution structure of the human Grb7-SH2 domain in complex with the 10 amino acid peptide pY1139
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Varian | INOVA | Varian INOVA | 500 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 3D HNCA |
| 10 | 1 | 1 | 2D HMQC-J |
| 11 | 1 | 1 | 3D CBCANH |
| 12 | 1 | 1 | 3D HCCH-TOCSY |
| 13 | 1 | 1 | 13C, 15N→12C, 14N NOESY |
| 14 | 1 | 1 | 12C, 14N→13C, 15N NOESY |
| 15 | 1 | 1 | 12C, 14N→12C, 14N NOESY |
| 16 | 1 | 1 | 12C, 14N→12C, 14N TOCSY |
| 2 | 1 | 1 | 3D HN(CO)CA |
| 3 | 1 | 1 | 3D HNCACB |
| 4 | 1 | 1 | 3D CBCA(CO)NH |
| 5 | 1 | 1 | 2D 15N HSQC |
| 6 | 1 | 1 | CN NOESY-HSQC |
| 7 | 1 | 1 | 3D 15N NOESY-HSQC |
| 8 | 1 | 1 | 3D 13C NOESY-HSQC |
| 9 | 1 | 1 | 3D TOCSY-HSQC |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 6.6 | ambient | 298 |
Conformers
| Conformers Calculated Total Number | 50 |
| Conformers Submitted Total Number | 10 |
