2L29

Complex structure of E4 mutant human IGF2R domain 11 bound to IGF-II

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Varian	INOVA	Varian INOVA	600
2	Varian	VNMRS	Varian VNMRS	600
3	Varian	UNITYPLUS	Varian UnityPlus	900

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	2	3D 1H-13C NOESY
10	1	1	3D CBCA(CO)NH
11	1	1	3D C(CO)NH
12	1	1	3D HNCA
13	1	1	3D HNCACB
14	1	1	3D HNCACB
15	1	1	3D HCCH-TOCSY
16	1	1	3D HN(CO)CA
17	1	1	3D H(CCO)NH
18	1	1	3D 1H-15N NOESY
19	1	1	3D 1H-13C NOESY
2	1	1	3D 1H-15N NOESY
20	1	2	2D 1H-15N HSQC
21	1	2	2D 1H-13C HSQC
22	1	2	3D CBCA(CO)NH
23	1	2	3D C(CO)NH
24	1	2	3D HNCO
25	1	2	3D HNCA
26	1	2	3D HNCACB
27	1	2	3D HN(CO)CA
28	1	2	3D H(CCO)NH
29	1	2	3D HCCH-TOCSY
3	1	1	3D 1H-15N NOESY
30	1	2	3D 1H-15N NOESY
31	1	2	3D 1H-13C NOESY
32	1	1	2D f2 filter noesy
33	1	2	2D f2 filter noesy
34	1	1	2D f2 filter noesy
35	1	2	2D f2 filter noesy
36	1	1	2D CN filtered noesy
37	1	2	2D CN filtered noesy
38	1	1	2D CN filtered noesy
39	1	2	2D CN filtered noesy
4	1	2	3D 1H-13C NOESY
40	1	1	2D CN filtered tocsy
41	1	2	2D CN filtered tocsy
5	1	3	2D 1H-15N HSQC
6	1	3	3D 1H-15N NOESY
7	1	1	2D 1H-15N HSQC
8	1	1	2D 1H-13C HSQC
9	1	1	3D HNCO

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	4.2	ambient	310

Conformers

Conformers Calculated Total Number	200
Conformers Submitted Total Number	20