2KYV

Hybrid solution and solid-state NMR structure ensemble of phospholamban pentamer

Spectrometer

Experimental method: SOLID-STATE NMR, SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Varian	VXRS	Varian VXRS	600
2	Bruker	ARX	Bruker ARX	600
3	Varian	INOVA	Varian INOVA	800

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
2	1	1	3D 1H-15N NOESY
3	1	1	2D 1H-13C HSQC
4	2	2	PISEMA
5	2	2	SAMPI4

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6	ambient	310
2			278

Conformers

Conformers Calculated Total Number	200
Conformers Submitted Total Number	20