2KW6
Solution NMR Structure of Cyclin-dependent kinase 2-associated protein 1 (CDK2-associated protein 1; oral cancer suppressor Deleted in oral cancer 1, DOC-1) from H.sapiens, Northeast Structural Genomics Consortium Target Target HR3057H
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | AVANCE | Bruker Avance | 800 |
| 2 | Varian | INOVA | Varian INOVA | 600 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 2D 1H-15N HSQC |
| 10 | 1 | 1 | 3D HCCH-TOCSY |
| 11 | 1 | 1 | 3D HCCH-COSY |
| 12 | 1 | 1 | 2D 1H-15N hetNOE |
| 13 | 1 | 1 | 3D HNCACB |
| 14 | 1 | 1 | 3D HN(CA)CO |
| 15 | 1 | 1 | 3D CBCA(CO)NH |
| 16 | 1 | 1 | 3D HNCACB |
| 17 | 1 | 2 | 2D 1H-13C HSQC high res. (L/V methyl stereospecific assignment) |
| 18 | 1 | 2 | 2D 1H-15N T1 relaxation |
| 19 | 1 | 2 | 2D 1H-15N T2 relaxation |
| 2 | 1 | 1 | 2D 1H-13C HSQC |
| 20 | 1 | 2 | 2D 1H-15N hetNOE |
| 21 | 1 | 3 | X-filtered 13C NOESY |
| 22 | 1 | 4 | 2D 1H-15N TROSY |
| 23 | 1 | 5 | 3D HNCO |
| 3 | 1 | 1 | 3D simutaneous 13C-aromatic,13C-aliphatic,15N edited 1H-1H NOESY |
| 4 | 1 | 1 | 3D HNCO |
| 5 | 1 | 1 | 3D HBHA(CO)NH |
| 6 | 1 | 1 | 2D 1H-13C arom NOESY |
| 7 | 1 | 1 | 3D HCCH-TOCSY |
| 8 | 1 | 1 | 3D HNCA |
| 9 | 1 | 1 | 3D HN(CO)CA |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 6.5 | ambient | 298 |
Conformers
| Conformers Calculated Total Number | 100 |
| Conformers Submitted Total Number | 20 |
